Adding a certain compound to certain chemical reactions, such as: 5020-41-7, 2-(3-Methoxyphenyl)ethanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, 5020-41-7, blongs to alcohols-buliding-blocks compound. Recommanded Product: 5020-41-7
General procedure: All reactions were conducted in a 10-mL V-type vessel equipped with a triangular magnetic stirrer. In a typical reaction, 2-(3,4-dimethoxyphenyl)ethanol (91.1 mg, 0.5 mmol), benzaldehyde (64.8 mg, 0.6 mmol), and 1b (10 mg, 1 mol%) were mixed in 1,2-dichloroethane (1.0 mL) and stirred for 5 h at 80 C. After the reaction, the mixture was cooled to room temperature and then centrifuged, and the liquid phase was subjected to isolation with PTLC (eluting solvent: ethyl acetate/petroleum ether = 1/8). The desired product, 7a, was obtained in a yield of 96%. Tests of the substrate scope were conducted in the same manner. The recycling of 1b was realized after doubling the dose. After washing the solid phase with PE (3.0 mL × 3) and drying under vacuum, the recovered 1b was used in the next run with a similar procedure.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,5020-41-7, its application will become more common.
Reference:
Article; Zeng, Kexing; Huang, Zhipeng; Yang, Jie; Gu, Yanlong; Cuihua Xuebao/Chinese Journal of Catalysis; vol. 36; 9; (2015); p. 1606 – 1613;,
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