Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 186020-66-6, name is tert-Butyl 12-Hydroxy-4,7,10-trioxadodecanoate. This compound has unique chemical properties. The synthetic route is as follows. Quality Control of tert-Butyl 12-Hydroxy-4,7,10-trioxadodecanoate
Step b: The crude product from step a (40.23 g, 0.157 mol) was dissolved in 50 mL pyridine, cooled to 0 C., and Ts-Cl (32.92 g, 0.173 mol) was added slowly. The flask containing the reaction mixture was sealed and placed in a refrigerator at 0 C. for 24 h. The reaction mixture was poured into ice/H2O, and the aqueous layer was extracted with CH2Cl2 (3×100 mL). The combined organic layers were washed with 2% HOAc in H2O, and dried over anhydrous MgSO4. The solvent was removed under vacuum to yield the tosylate as colorless oil. The oil was dried under vacuum (52.97 g, mol, 78%). HPLC: tR=13.0 min.
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Reference:
Patent; Wilbur, D. Scott; Pathare, Pradip M.; Hamlin, Donald K.; Wan, Feng; US2006/228325; (2006); A1;,
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