Reference of 217479-60-2, Adding some certain compound to certain chemical reactions, such as: 217479-60-2, name is 2,4,6-Trichlorobenzyl alcohol,molecular formula is C7H5Cl3O, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 217479-60-2.
To a stirred solution of 2,4,6-trichlorobenzylalcohol (10.0 g; 47.3 mmoles) in chloroform (100 ml) kept under nitrogen atmosphere, thionyl chloride (6.07 mL, 85.1 mmole) was added slowly at 0 C. over a period of 15 minutes followed by catalytic amount of DMF. The reaction mix was allowed to stir at ambient temp for 3 hours. The reaction mixture was quenched with 50 mL of water; the aqueous layer was extracted with DCM (3*100 ml). The combined organic layer was washed with 5% sodium bicarbonate solution (2*50 ml) followed by brine (50 ml) and dried over anhydrous sodium sulphate. The solvent was evaporated under reduced pressure. 10.9 g (100.0% of theory) of 1,3,5-trichloro-2-chloromethyl-benzene was obtained in form of a white solid. 1HNMR (CDCl3, 400 MHz): delta=7.37 (2H, s); 4.82 (2H, s) Mass: M=229.8
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 217479-60-2, 2,4,6-Trichlorobenzyl alcohol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; SYNGENTA CROP PROTECTION LLC; US2011/230537; (2011); A1;,
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