Electric Literature of 2516-33-8, In the chemical reaction process,reaction time,type of solvent,can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product.An updated downstream synthesis route of 2516-33-8 as follows.
EXAMPLE 3 Cyclopropanecarboxyaldehyde, 2-(1-nonenyl)-,(Z)- A solution of cyclopropanemethanol, 2-(1-nonenyl)-, (21.6 g, 0.11 moles) in methylene chloride (25 ml) is added dropwise to a solution of pyridinium dichromate (79.8 g, 0.208 moles) in methylene chloride (200 ml) at room temperature under nitrogen. The reaction mixture is stirred overnight. The mixture is diluted with ether (500 ml), filtered through celite and then through a short column of silica gel. The solvents are stripped from the filtrate to give the crude product (21.6 g). Distillation at reduced pressure gives the product as a clear colorless oil (14.8 g, 69%), b.p. 81-86 C. (0.06 mm).
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,2516-33-8, its application will become more common.
Reference:
Patent; Warner-Lambert Company; US4562006; (1985); A;,
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