Related Products of 1562-00-1, Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 1562-00-1, name is Sodium isethionate. A new synthetic method of this compound is introduced below.
800 g (10.3 mol) of a 40% methylamine aqueous solution,WhenSodium isethionate509 g (3.4 mol)Was charged in an autoclave having a capacity of 2 liters,The reaction was carried out at 200 to 250 C. under a pressure of 20 kg / cm 2 for 5 to 7 hours.After cooling, the excess methylamine was recovered by distillation, the residue was concentrated and evaporated to dryness.The reaction product was mixed with 2500 g of a mixed solvent of dimethylformamide and water(Mass ratio of dimethylformamide / water = 2/1)To obtain a compound of the formula (1).The yield was 228 g.In the resulting compound of formula (1), M is sodium.
At the same time, in my other blogs, there are other synthetic methods of this type of compound,1562-00-1, Sodium isethionate, and friends who are interested can also refer to it.
Reference:
Patent; NOF Corporation; Matsuo, Satoshi; Fujita, Hiroya; (13 pag.)JP6103210; (2017); B2;,
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