New downstream synthetic route of Mesitylmethanol

At the same time, in my other blogs, there are other synthetic methods of this type of compound,4170-90-5, Mesitylmethanol, and friends who are interested can also refer to it.

Adding a certain compound to certain chemical reactions, such as: 4170-90-5, Mesitylmethanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, name: Mesitylmethanol, blongs to alcohols-buliding-blocks compound. name: Mesitylmethanol

In the glove box, Mn(CO)5Br (0.005mmol),[(E)-2-(2-(1-(2-pyridyl)ethylidene)-indenyl)pyridin](0.006mmol),Add 1.0 mL of toluene, stir for two hours, add 2-methylquinoline 4 (2 mmol)2e (1mmol), after reacting at 135 C for 48 hours, the reaction was stopped, and the solvent was evaporated to dryness.Column chromatography ethyl acetate / petroleum ether (1:10),Trans-disubstituted olefin derivative 3ae. The product was a white solid in 80% yield.

At the same time, in my other blogs, there are other synthetic methods of this type of compound,4170-90-5, Mesitylmethanol, and friends who are interested can also refer to it.

Reference:
Patent; Qingdao University of Science and Technology; Zhang Chunyan; (19 pag.)CN108250153; (2018); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts