In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 153599-45-2, name is Methyl 3-(2-hydroxyethyl)benzoate, the common compound, a new synthetic route is introduced below. Application In Synthesis of Methyl 3-(2-hydroxyethyl)benzoate
3- (2-HYDROXYETHYL)- benzoic acid methyl ester (50 mg, 0.28 mmol) was dissolved in methanol (1 ml). 1N NaOH aqueous solution (1 ml) was added therein. The reaction mixture was stirred at room temperature for 1 hour to give 43 mg (yield: 95%, white solid) of the target compound. 1H NMR (400MHZ, CDC13) ; 52. 32 (br, 1H), 2.89 (t, J=6. 4Hz, 2H), 3.85 (t, J=6. 4Hz, 2H), 7.36 (t, J=7. 6Hz, 1H), 7.42 (D, J=5. 6Hz, 1H), 7.88 (d, J=8. 8Hz, 1H), 7.89 (s, 1H)
The synthetic route of 153599-45-2 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; JE IL PHARMACEUTICAL CO., LTD.; WO2004/113281; (2004); A1;,
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