Sources of common compounds: 1-Adamantaneethanol

According to the analysis of related databases, 6240-11-5, the application of this compound in the production field has become more and more popular.

Reference of 6240-11-5, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 6240-11-5, name is 1-Adamantaneethanol. This compound has unique chemical properties. The synthetic route is as follows.

1- Adamantane ethanol (4.758 g, 26.4 mmol, Aldrich, Milwaukee, WI) was added, and the sealed mixture was stirred overnight at room temperature. It was then poured into 10% NaHCO3 solution (50 mL) and the pyridine was evaporated under vacuum. The slightly yellow solid was dissolved in 1 L of water and extracted with ether (three 150 mL portions). The aqueous phase was acidified with 2 N HCl to pH 1, and then extracted with three 150 mL portions of CHCl3 :H-BUOH (7:3). The combined organic layer (ether and CHCl3 :w-BuOH) was washed with water and a slightly yellow precipitate was formed in the mixed solvents, at which point the solvents were evaporated under vacuum. A slightly yellow solid was formed and was recrystallized from acetone/hexane. The solid was dried under vacuum, yield 60 %

According to the analysis of related databases, 6240-11-5, the application of this compound in the production field has become more and more popular.

Reference:
Patent; INSERT THERAPEUTICS, INC.; WO2006/89007; (2006); A2;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts