The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 13330-96-6, name is 4-(Dimethylamino)butan-1-ol. This compound has unique chemical properties. The synthetic route is as follows. Recommanded Product: 4-(Dimethylamino)butan-1-ol
Example S. Synthesis of MC4 Ether.[0294] MC4 Ether (Compound 15) having the structure shown below was synthesized as described below.Chemical Fotmuta: Omicron^Eta,, OmicronExact Mass: 627.6Molecular Wteirjit 628.1Bemena And sis: C.8222; K 13.00; N, 2.23; 0.2.55MC4 Ether[0295] A 50 mL RBF with stir-bar were flushed with nitrogen, and NaH (220 mg, 9 mmol), dimethylaminobutanol (1.05g, 9 mmol) and anh. benzene (10 mL) added. Aftereffervescence subsided, Compound 14 (440 mg, 0.75 mmol) was added and RM refluxed overnight at 90C. TLC indicated some product formation. The reaction was diluted to 40 mL with benzene, and quenched with ethanol (25 mL). It was then washed with water (40 mL), dried and concentrated. The crude product was purified to yield product as a pale yellow oil, 145 mg, 31%.
With the rapid development of chemical substances, we look forward to future research findings about 13330-96-6.
Reference:
Patent; PROTIVA BIOTHERAPEUTICS, INC.; HEYES, James; WOOD, Mark; MARTIN, Alan; WO2011/141705; (2011); A1;,
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