Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 7073-69-0, name is 2-(2-Bromophenyl)propan-2-ol. This compound has unique chemical properties. The synthetic route is as follows. COA of Formula: C9H11BrO
In a 250mL three-neck bottle,Under the protection of nitrogen,Add 0.03 mol of dibenzofuran-3-amine,0.04 mol of 2-(2-bromophenyl)propan-2-ol,150mL toluene was stirred and mixed,Then add 0.05 mol of sodium t-butoxide,0.0015mol Pd2 (dba)3,0.0015 mol of tri-tert-butylphosphine, heated to 115 C,Reflow reaction for 24 hours;Naturally cooled to room temperature, filtered, and the filtrate was subjected to vacuum distillation (-0.09 MPa, 85 C), and passed through a neutral silica gel column.Obtaining 2-(2-(dibenzofuran-3-ylamino)phenyl)propan-2-ol;
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Reference:
Patent; Jiangsu March Optoelectric Technology Co., Ltd.; Miao Kangjian; Zhang Zhaochao; Zhang Xiaoqing; Li Chong; (48 pag.)CN108203428; (2018); A;,
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