Reference of 101597-25-5, Adding some certain compound to certain chemical reactions, such as: 101597-25-5, name is 1,1-Bis(4-methoxyphenyl)prop-2-yn-1-ol,molecular formula is C17H16O3, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 101597-25-5.
To the vial tube, 5-hydroxy-7,7,13,13-tetramethyl-7H, 13H-benzo [g] indeno [3,2-b] fluorene (8) (50 mg, 0.13 mmol)1,1-bis (4-methoxyphenyl) prop-2-yl-1-ol (9) (35 mg, 0.13 mmol)P-Toluenesulfonic acid monohydrate (1.0 mg, 0.0053 mmol) was added,Sealed with a Teflon (registered trademark) septum cap, purged with nitrogen and toluene (1.3 mL) was added,And the mixture was stirred at 0 C. for 12 hours.Progress of the reaction was confirmed by TLC (hexane / ethyl acetate = 9/1)After confirming the completion of the reaction, the reaction was terminated with an aqueous solution of sodium hydrogencarbonate, and extraction was carried out using ethyl acetate. The extracted organic layer was dried over magnesium sulfate, filtered, and concentrated. The obtained crude product was isolated and purified by silica gel column chromatography (hexane / ethyl acetate = 19/1 to 9/1) to give 64 mg (77%)of3,3-di (4-methoxyphenyl) -10, 10, 16,16-tetramethyl-3H, 10H, 16H-benzo [3,4] indeno [2 ‘, 3’: 6,7] fluoreno [1,2-b] pyran(10) as a dark green solid.
According to the analysis of related databases, 101597-25-5, the application of this compound in the production field has become more and more popular.
Reference:
Patent; TOSOH ORGANIC CHEMICAL COMPANY LIMITED; KITO, FUKASHI; HAGIWARA, HIDEKI; SOGA, SHINICHI; (20 pag.)JP2017/36248; (2017); A;,
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