Adding a certain compound to certain chemical reactions, such as: 647-42-7, 3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctan-1-ol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Quality Control of 3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctan-1-ol, blongs to alcohols-buliding-blocks compound. Quality Control of 3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctan-1-ol
General procedure: A two-necked, 500-mL round bottom flask was equipped with a magnetic stirring bar and a three-way stopcock, of which one way was connected to an argon flow line and the other was connected to a vacuum line. The apparatus was flame-dried in vacuum, and allowed to cool to room temperature under an argon purge. To a solution of [IrCl(cod)]2 (1 mol%) in dry toluene triethylene glycol monomethyl ether, vinyl acetate (2.0 equiv), and Na2CO3 (0.60 equiv) were added and the mixture was stirred at 100 C for 3 h. After the reaction, the resulting salts were removed and washed with Et2O. The solvent was removed under reduced pressure. Purification of the residue by vacuum distillation (2 times distillation with CaH2) gave the product.
The synthetic route of 647-42-7 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Harada, Nari-Aki; Nishikata, Takashi; Nagashima, Hideo; Tetrahedron; vol. 68; 15; (2012); p. 3243 – 3252;,
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