Related Products of 110-73-6, Adding some certain compound to certain chemical reactions, such as: 110-73-6, name is 2-(Ethylamino)ethanol,molecular formula is C4H11NO, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 110-73-6.
General procedure: All compounds were prepared according our previous works[12]. The general procedure: Amines (1 mmol) was dissolved in20 mL of MeOH. Equal molar NaOH aqueous solution was added to the methanol solution. Excess CS2 was slowly dropped into thereaction flask in an ice bath. The reaction was completed at roomtemperature for 8 h. The solution was then evaporated and theresidue was precipitated three times with diethyl ether and filtered and dried to give a white powder product. All sodium dithiocarbamate(A1-22) are white solid. A1-22 and equal molar Mn(CO)5Brwere dissolved in 15mL of methanol. The solution immediately became yellow and was stirred at room temperature for 3 h. Thesolution was then evaporated and the yellow residue was dissolved in Ether. The solution was placed in 2-4 C for 2 h and the supernatant was evaporated to give a yellow solid. After recrystallization three times with DCM and CYH, the final product was obtained.
According to the analysis of related databases, 110-73-6, the application of this compound in the production field has become more and more popular.
Reference:
Article; Bai, Zhongjie; Zhang, Jinlong; Zhang, Qiuping; Zhang, Taofeng; Li, Jili; Zhao, Quanyi; Wang, Zhen; He, Dian; Cheng, Jie; Zhang, Jingke; Liu, Bin; European Journal of Medicinal Chemistry; vol. 159; (2018); p. 339 – 356;,
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