Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 589-98-0, name is 3-Octanol. This compound has unique chemical properties. The synthetic route is as follows. name: 3-Octanol
1.31 g (10.1 mmol) of 3-octanol,0.170 g (0.50 mmol) of tetrabutylammonium hydrogensulfate and 0.0155 g (0.10 mmol) of TEMPO were dissolved in 30 mL of dichloromethane and charged into the reaction vessel. After the liquid temperature in the reaction vessel was cooled to 5 DEG C, 1.98 g (12.0 mmol) of the crystals of sodium hypochlorite pentahydrate was added with stirring, and then the liquid temperatureThe mixture was kept at 5 DEG C and stirredOxidation reaction was carried out. After 1 hour from the start of the oxidation reaction, internal standard analysis was carried out by GC in the same manner as in Example 1 to find that 3-octanone was produced at a yield of 97%.
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Reference:
Patent; NIPPON LIGHT METAL COMPANY, LIMITED; TOMOHIDE, OKADA; TOMOTAKE, ASAWA; YUKIHIRO, SUGIYAMA; (9 pag.)KR2015/26729; (2015); A;,
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