Adding a certain compound to certain chemical reactions, such as: 5333-42-6, 2-octyldodecan-1-ol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Recommanded Product: 2-octyldodecan-1-ol, blongs to alcohols-buliding-blocks compound. Recommanded Product: 2-octyldodecan-1-ol
Take 0.1g (452g/mol, 0.22mmol)Diisobutyl 3,9-nonanedicarboxylate in a round bottom flask, adding 1.63g(298 g/mol, 5.5 mmol) of 2-octyldodecanol was heated to 100 C,Add 0.01 g (10 wt%) of dihydroxybutyl tin chloride to the reaction flask,The temperature was raised to 170 C, and the reaction was heated for 3 h, and the plate was tracked during the reaction.After the reaction, the reaction was cooled to room temperature and the temperature was raised to 180 C.Vacuum distillation,Distilling off excess 2-octyldodecanol which acts as both a solvent for the reaction and a reactantDry in vacuum. The resulting product was cooled to room temperature and dissolved in petroleum ether.The wet method was purified by silica gel column to obtain a yellow dye. The conversion was calculated to be 90%.
The synthetic route of 5333-42-6 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Shenzhen Guohua Optoelectric Technology Co., Ltd.; Shenzhen Guohua Optoelectric Institute; Zhou Guofu; Deng Yong; Li Shi; Ye Dechao; (8 pag.)CN109627802; (2019); A;,
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