Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 505-10-2, name is 3-(Methylthio)propan-1-ol. A new synthetic method of this compound is introduced below., COA of Formula: C4H10OS
The mixture of the compound 46 (2.00g), meta-chloroperbenzoic acid (9.40g), and a methylene chloride (60 mL) was stirred at the room temperature for 16 hours. Reaction mixed liquor was concentrated in vacuum after cerite filtration, silica gel column chromatography (eluate: chloroform/methanol =9/1) refined residue, and it obtained the compound 47 (0.660g).
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Reference:
Patent; SUMITOMO DAINIPPON PHARMA COMPANY LIMITED; Tsuzuki, Yasunori; Komiya, Masafumi; Furuta, Tomoyuki; Iwamoto, Kohei; Takahashi, Yoko; Nonoyama, Akihito; (130 pag.)JP2017/1991; (2017); A;,
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