Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 583-03-9, name is 1-Phenylpentan-1-ol. This compound has unique chemical properties. The synthetic route is as follows. Recommanded Product: 583-03-9
In a typical reaction, acetic anhydride (500muL, 5.3mmol), pyridine (200muL) and triethylamine (4.0mmol) were added subsequently to a stirred solution of 1-phenylpentanol rac-4a (492mg, 3.0mmol) in dichloromethane (2mL) at room temperature. The reaction was stirred for 24h-52h at room temperature, monitored by TLC. Dichloromethane (10mL) was added and the mixture was quenched with an addition of 1M aq HCl (2mL). The aqueous layer was extracted with dichloromethane (2¡Á10mL). The combined organic extracts were neutralized and washed with saturated aq NaHCO3 (5mL) and brine (10mL), then dried over MgSO4 and filtered. The organic solvent was concentrated under reduced pressure and the residue was purified by silica gel column chromatography (hexane/ethyl acetate, 3:1) to give corresponding acetate rac-4b. The 1H NMR spectra of acetates 3b,24 4b,24 5b,24 6b,24 7b,26 8b,28 9b29 were all in agreement with those reported in the literature.
If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it, 583-03-9, 1-Phenylpentan-1-ol.
Reference:
Article; Hoang, Hai Nam; Matsuda, Tomoko; Tetrahedron; vol. 72; 46; (2016); p. 7229 – 7234;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts