Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 114686-85-0, name is 2-(2,3-Dichlorophenyl)ethanol. This compound has unique chemical properties. The synthetic route is as follows. Application In Synthesis of 2-(2,3-Dichlorophenyl)ethanol
A mixture of 2-(2,3-dichlorophenyl)ethanol (0.50 g), NaHCO3 (0.438 g) and Dess-Martin periodinane (1.22 g) in dichloromethane (10 mL) and water (46 mL) was stirred for 1 hour. The mixture was quenched with aqueous NaHCO3 and saturated aqueous Na2S2O3 and extracted with dichloromethane. The extract was dried (Na2SO4), filtered and concentrated. The concentrate was purified on silica gel with an Intelliflash-280 purification system with hexanes/ethyl acetate.
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Reference:
Patent; Sheppard, George S.; Wang, Gary T.; Palazzo, Fabio; Bell, Randy L.; Mantei, Robert A.; Wang, Jieyi; Hubbard, Robert D.; Kawai, Megumi; Erickson, Scott A.; BaMaung, Nwe; Fidanze, Steve D.; US2007/203143; (2007); A1;,
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