In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 3597-91-9, name is [1,1′-Biphenyl]-4-ylmethanol, the common compound, a new synthetic route is introduced below. Quality Control of [1,1′-Biphenyl]-4-ylmethanol
In a 10 mL round bottom flask, 0.85 g of 4-hydroxymethylbiphenyl (4-phenylbenzyl alcohol) and 2 g of diethylene glycol dimethyl ether were sequentially added, and the resulting mixture was subjected to an ultrasonic reaction apparatus at 40 KHz/30 W/70. C Ultrasonic radiation was allowed to open for 35 minutes. The diethylene glycol dimethyl ether was removed under reduced pressure, and recrystallized to give 0.95 g of 4-phenylbenzoic acid, yield 96%.
The synthetic route of 3597-91-9 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Central South University; Xiao Fang; Xiao Yuanyuan; Zeng Ming; Li Na; Yin Lirong; (15 pag.)CN108467342; (2018); A;,
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