Reference of 3344-77-2, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 3344-77-2, name is 12-Bromododecan-1-ol, molecular formula is C12H25BrO, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
(a) 2-(12-Bromododecyloxy)tetrahydropyran 12-Bromo-dodecan-1-ol (5.12 g, 19.3 mmol) was added to a vigorously stirred solution of dihydropyran (2.1 mL, 23.2 mmol) and Amberlyst HI5 (0.25 g, Aldrich D10,620-8) in hexane (100 mL). After 3 hours dihydropyran (2.1 mL) was added and the solution stirred for a further 15 hours. The mixture was then filtered, and the filtrate concentrated in vacuo and chromatographed graphed on silica gel, eluding with 2percent ethyl acetate in hexane to give the title compound, (a), 8.02 g (75percent), as an oil.
According to the analysis of related databases, 3344-77-2, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Warner-Lambert Company; US5073565; (1991); A;,
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