Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 115-20-8, name is Trichloroethanol. This compound has unique chemical properties. The synthetic route is as follows. SDS of cas: 115-20-8
Compound 1 (2g, 13.4mmol) was dissolved intetrahydrofuran (15ml) was added triethylamine (176mg), Was added dropwise to asolution of compound 2 (2.1g, 24.8mmol), dropwise addition was heated to 60 C under reflux, stirringStirred overnight. The reaction was stopped, after the reaction mixture wascooled added saturated citric acid (20ml), extracted with methylene chloride,The organic layer was washed with water, brine, dried over anhydrous NaSO 4,isolated by column chromatography to give compound 3 (2.2g, 71% yield).
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Reference:
Patent; ARROMAX PHARMATECH SUZHOU CO LTD; JIAN, HONG; XU, XIN; (12 pag.)CN104230792; (2016); B;,
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