Electric Literature of 627-30-5, Adding some certain compound to certain chemical reactions, such as: 627-30-5, name is 3-Chloropropan-1-ol,molecular formula is C3H7ClO, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 627-30-5.
Example 5: Production of polymer particles by treating a mixture of azide-modified PAA and alkyne-modified PAA with acid; Synthesis of 3-azidopropanol: In a 100 ml_ round bottom flask, liquid 3- chloropropanol (10.0 g, 1.0 equiv), solid sodium azide (17.19 g, 2.5 equiv) were reacted in DMF for 40 hours at 100 0C. The reaction mixture was cooled to room temperature, poured into a reparatory funnel and extracted with diethyl ether (300 ml_) and brine solution (500 ml_). The organic layer was separated and dried over MgSO4. Rotary evaporation removed the diethyl ether solvent at room temperature and yielded crude 3-azidopropanol (12.5 g). 1H-NMR (delta, ppm) CDCI3: 3.76 – 3.73 (t, 2H, HOCH2CH2CH2N3), 3.46 – 3.43 (t, 2H, HOCH2CH2CH2N3), 2.09 (br-s, 1 H, OH), 1.86 – 1.80 (m, 2H, HOCH2CH2CH2N3). IR neat (cm”1): 2100 (N=N=N).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 627-30-5, 3-Chloropropan-1-ol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; VIVE NANO, INC.; LI, Fugang; PHAM, Hung; ANDERSON, Darren, J.; WO2010/35118; (2010); A1;,
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