Reference of 5187-23-5, Adding some certain compound to certain chemical reactions, such as: 5187-23-5, name is (5-Ethyl-1,3-dioxan-5-yl)methanol,molecular formula is C7H14O3, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 5187-23-5.
Example 24: Synthesis of Penta(cyclohexylamino)-mono(5-ethyl-1,3-dioxane-5- methyloxy)-decafluoro-phthalocyaninatozinc(II) [00164] FL6ZNPC (10 mg) was dissolved in 1-2 ml of cyclohexylamine and heated to 100C for 1 hour. The product was purified by silica gel chromatography using ethyl acetate as the eluent, and then added to a mixture of 1 ml 5-ethyl-1, 3-dioxane-5-methanol and 0.1 ml nBuLi, which had been stirred at room temperature for 15 minutes before. The whole reaction mixture was heated to 100-120C for 1 hour. The product was purified by silica gel chromatography using a mixture of hexanes : ethyl acetate = 1: 1 as the eluting solvent. A brown fraction was collected. The MALDI-MS shows the following substitution pattern: Cyclohexylamine 5-Ethyl-l, 3-dioxane-5-methanol nnlz 3 0 1100 4 0 1182 5 0 1261 4 1 1307 6 0 1338 5 1 1387 4 2 1432 5 2 1513 [00165] The reaction scheme for the synthesis of this product is provided in Figure 19.
According to the analysis of related databases, 5187-23-5, the application of this compound in the production field has become more and more popular.
Reference:
Patent; YORK UNIVERSITY; WO2005/33110; (2005); A1;,
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