Related Products of 5675-51-4, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 5675-51-4, name is 1,12-Dodecanediol, molecular formula is C12H26O2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
Example 1 Preparation of 12-bromododecan-1-ol (3) 48% HBr in water (77 ml; 0.46 mol; 15 eq.) is added to a solution of 1,12-dodecan-ol (6.15 g; 30.4 mmol; 1 eq.) in cyclohexane (140 ml). The heterogeneous mixture is heated under reflux. After 6 h, the aqueous phase is extracted with ether (3*100 ml). The organic phases are combined, washed with a saturated solution of Na2CO3, dried on MgSO4, filtered and evaporated. The crude reaction product is purified by silica gel chromatography (eluent: hexane-AcOEt: 6-4) to yield 7.06 g of a white solid. Yield: 85% Empirical formula: C12H25BrO
According to the analysis of related databases, 5675-51-4, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Centre National de la Recherche Scientifique(CNRS); Universite de Luxembourg; US2010/48731; (2010); A1;,
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