3360-41-6, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 3360-41-6, name is 4-Phenylbutan-1-ol. This compound has unique chemical properties. The synthetic route is as follows.
Triphenylphosphine (2.72 g, 10.4 mmol) was added to the 4-phenyl-1-butanol (1.2 g, 8.0 mmol) in CCl4 (10 mL) at room temperature under atmosphere of argon, and the mixture was refluxed for 1 h. The reaction quenched with water and extracted with hexane. The extracts were washed with brine, dried over MgSO4, and concentrated under reduced pressure. The residue was purified by column chromatography with hexane/AcOEt (100:1) to give (4-chlorobutyl)benzene (5d) as a colorless oil in 85% yield. The analytical data were identical with those of a literature compound.10 IR (neat): nu = 2940 (CH2), 699 (Alkyl-Cl); 1H NMR (500 MHz, CDCl3): delta = 1.72-1.86 (4H, m), 2.64 (2H, t, J = 7.2 Hz), 3.54 (2H, t, J = 6.3 Hz), 7.15-7.21 (3H, m), 7.25-7.31 (2H, m); 13C NMR (125 MHz, CDCl3): delta = 28.5, 32.1, 35.1, 44.9, 125.9, 128.4, 141.8; MS (EI) m/z 168 ([M]+).
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Reference:
Article; Hatae, Noriyuki; Kujime, Eiko; Yano, Keigo; Kizuka, Mami; Ashida, Rina; Choshi, Tominari; Nishiyama, Takashi; Okada, Chiaki; Iwamura, Tatsunori; Yoshimura, Teruki; Heterocycles; vol. 97; 1; (2018); p. 560 – 568;,
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