1074-16-4, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 1074-16-4, name is 2-(2-Bromophenyl)ethanol. This compound has unique chemical properties. The synthetic route is as follows.
17.6 g (0.314 mol) KOH in 100 mL DMSO was placed in a flask fitted with dropping funnel and magnetic stirrer placed in water bath at ca. 7 C. A solution of 9.9 mL (22.57 g, 0.159 mol) of iodomethane and 13.94 g (0.0742 mol) of 2-(2-bromophenyl)ethanol in 80 mL DMSO was dropped-in while keeping the temperature 21-22 C. Water bath was removed and the reaction mixture was stirred for 2 h while the temperature raised to 27 C. After cooling to RT reaction mixture was poured into 600 mL of water, than extracted with diethyl ether (300 mL and 2 ¡Á 100 mL). Ether extract was washed with water (2 ¡Á 150 mL) and volatiles were distilled off to give 14.6 g of 2-bromo-(2-methoxyethyl)benzene (0.0679 mol, 91.5%), which was used without further purification. 1H NMR (400 MHz, CDCl3): delta: 3.08 (t, 2H), 3.42 (s, 3H), 3.66 (t, 2H), 7.10-7.14 (m, 1H), 7.26-7.33 (m, 2H), 7.57-7.59 ppm (m, 1H).
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 1074-16-4, 2-(2-Bromophenyl)ethanol.
Reference:
Article; Adamczyk-Wo?niak, Agnieszka; Brzozka, Zbigniew; Da?browski, Marek; Madura, Izabela D.; Scheidsbach, Roy; Tomecka, Ewelina; Zukowski, Kamil; Sporzy?ski, Andrzej; Journal of Molecular Structure; vol. 1035; (2013); p. 190 – 197;,
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