78-69-3, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 78-69-3, name is 3,7-Dimethyloctan-3-ol, molecular formula is C10H22O, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
Add 2g to the reaction flaskTetraacetyl substituted glucose bromine (chemical formula:), 0.38 g of tetrahydrolinalol (chemical formula:),0.73g of silver carbonate and 10mL of dichloromethane,Reacting at room temperature for 24 hours;The solvent was removed under reduced pressure.Separated by column chromatography,The eluent (a mixture of petroleum ether and ethyl acetate in a mass ratio of 5:1) was washed down with 0.80 g of a white solid.That is, tetrahydrolinalol tetraacetyl glucoside (chemical formula:).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 78-69-3, 3,7-Dimethyloctan-3-ol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Shanghai Institute of Technology; Li Hongyi; Pan Xianhua; Chen Yu; Huo Jiyou; Yuan Hongshun; (9 pag.)CN109970826; (2019); A;,
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