Sources of common compounds: 627-18-9

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 627-18-9, 3-Bromopropan-1-ol.

627-18-9, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 627-18-9, name is 3-Bromopropan-1-ol. This compound has unique chemical properties. The synthetic route is as follows.

In a 500 mL round-bottom flask, 3-bromopropan-1-ol (12.4 g, 89.2 mmol, 1 eq.) was dissolved in acetone (200 mL). A solution of sodium azide (29.0 g, 466 mmol, 5.2 e.) in deionized water (120 mL) was added while stirring. A catalytic amount of Kl (approximately 2 mg) was added. This solution was stirred at room temperature for 48 hours. After extraction with diethyl ether (3 x 80 mL), the combined organic layers were dryed over K2CO3. The drying agent was filtered off and the solvent evaporated in vacuo to give 3-azidopropan-1-ol as a highly viscous colourless oil (8.09 g, 80.0 mmol, 90 %). HRMS ESI(+) (MeOH) calculated for [M+Na]+: 124.04813, found: 124.04790.

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 627-18-9, 3-Bromopropan-1-ol.

Reference:
Patent; Universitaet Zuerich; GADEMANN, Karl; BERG, Regina; MEIER, Andrea; (43 pag.)EP3508492; (2019); A1;,
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