Adding a certain compound to certain chemical reactions, such as: 23147-58-2, Glycerol aldehyde dimer, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, 23147-58-2, blongs to alcohols-buliding-blocks compound. 23147-58-2
A mixture of final compound 2 (prepared according to Bl. b) (0.001 mol, 0.5 g), 1,4- dioxane-2,5-diol (0. 001 mol, 0.113 g) and 3-thiophene boronic acid (0. 001 mol, 0.106 g) in ethanol (5 ml) was stirred at room temperature for 18 hours. This was followed by addition of solution OF KC03 (10 %) and extracted with ethyl acetate. The combined organic layers were dried (MgSO4), filtered and concentrated under vacuum. The residue (0.6 g) was purified by column chromatography over silica gel (eluent: CH2Cl2/MeOH/NH40H 93/07/0.5) and the product fractions were concentrated. Yield: 0.075 g (12 %) of final compound 349.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,23147-58-2, its application will become more common.
Reference:
Patent; JANSSEN PHARMACEUTICA N.V.; WO2004/56799; (2004); A2;,
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